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Research Project

Superalloys

Microstructural evolution and grain boundary engineering.

Project Description

This project focuses on the microstructural evolution, phase stability, and grain boundary engineering in advanced Ni-based superalloys designed for high-temperature applications. Through a combination of thermo-mechanical processing, sub-solvus heat treatments, and multi-scale characterization techniques—including Atom Probe Tomography (APT), Transmission Electron Microscopy (TEM), Electron Backscatter Diffraction (EBSD), and in-situ X-ray diffraction—we investigate key phenomena such as γ/γ′ phase transformations, inverse precipitation, grain boundary engineering, and stress relaxation behavior. Particular emphasis is placed on solute segregation dynamics, the formation of heteroepitaxial interfaces, and the role of lattice misfit and crystallographic orientation relationships in influencing mechanical properties and long-term stability. These insights aim to support the design and optimization of next-generation superalloys with improved strength, corrosion resistance, and thermal stability for critical aerospace and energy applications.

Project Gallery

Related Publications

"Nucleation mechanism of hetero-epitaxial recrystallization..."

Scripta Materialia • Jan 2021

This study examines the formation of γ-like shells around primary γ′ precipitates in the AD730™ Ni-based superalloy...

"Chemical redistribution and change in crystal lattice parameters..."

Acta Materialia • Sept 2022

This study investigates the macroscopic contraction and stress relaxation retardation in γ/γ′ Ni-based superalloy AD730™...

"Microstructural characterization of three different size..."

Materials Characterization • Nov 2021

This study investigates phase evolution in a non-equiatomic nanocrystalline CoCuFeMnNi alloy...

"Role of carbide precipitates and process parameters..."

Metallurgical and Materials Transactions A • Oct 2015

This study explores thermo-mechanical processing routes to develop a grain boundary engineered (GBE) microstructure in alloy 617...